论文简介
E AT8w00016uA1e 1)>/w06;0102000Ae μ0 6 E日"29 &4i2⑥.EOAABO94U0010uA1e 1e/2> A14E6/%01x6EoAo£0A1 a3E219e↑°2A91u0y2"1++10μ° 6NS>" 7Ng1o31Tμ2+°2↔710072@O@O@9UE6AE PE μA1ele/%》A0-Ai j02AATjtca0O;t10+ i6°Ti0δE0εxo36AE 1uAU1a2i -0μA XLPE DOAUE-0。36AE a0U1E1a91-c01C3° if10/40 E elefk00|E%>ASEPE0D1w4-0Aa9AE9Q325. 12 TATxteETAeA TAOAtaRAE9ol - 94568 2000206 - 0041-06Recent Advances of Silane Crosslinking Technology for PEZUO Rui-linZHANG Guang- chengfHE Hong- weiEtIANG Guo-zhengf"Dept. of Chemistry EngineeringfNIUEXian 7100722@Abstract9he principleEmaterialsEtechnologyErharacterization and influncing factors of silane grafting andmoisture crosslinking for PE are described. Properties of some domnestically and interationally made XLPE are intro-duced . Present problems and prospect of XLPE are involved .Keywords&Silanefgraferosslink£PEPF2 ( CH2i@CH2无iECTBDT>0A0 o0SA~ μA_ ,B -0x0DOA: I0ia. Bif/%>A TEμiEi>" uata>~ 2> '6E物》ARqE_ BE->-9TT1E-0x0A- EaE3 j@P/%iEA^~\alWa9TA!TAE 95C~ 100CiE-0x0Ai1s 20 1oμA PE Ai. ,δ-0x0f".MμA>A|fE6E1 AaA1TADO2TjfPE. ,ADOμA00 -/hTooA-E15%6100D 12~ 13。δ1eleμ¥ la6u00e 1)>= PE μA0>%-* a_BAIEEDOLZEE; Ik>A@uA -%YE%Ecia, B PE AIE)2>A@uaWa%a' 6£6000 i@Sij@Oi@/u0ej@Si @Cj@ V4uμAEaDOμAx T/ota 1/-0.32112AC° PE μA1>A@ iEW"1y -oEaDORAθo 'E XLPE μAAIμI1ADO°ALyE0U - 50C>0 - 70CY2>胆." ityNo>-个/%>A -" ie e/>> .* μEA Eμ1021jf0e00ETE10Ajf2qC0EGE0U1e/>>A胆PE μA -0x0/a112>> iEaEu -/h- TatE£t1ele/%>A@ PE" XLPEODEqTAOAμa2314i2 .0*32>7 NS%>A@DjsEμA -0x0/aj@cj@Ci AW>AvyQGEhaEyf" 1fet。fqxEEUZ6uZuDSAE. βBE≈E +业μ1ε》.。01eNo>U%ujE00/hoDDE@/aE6°T- ”0|&AU1>DisEAcia1o2"2f0a01"0A0CiEEOAOUEtODAOqEμA PEfOaEEOAx V>Ac0o”EEuμAE >DμD0A0O》0A0U%B0DjPCj目00"62i -00Di1r3aATμA PEE》CiFE}Aa%ha11μA>- NS)>A= PEi&i%4E11ele}%<>A回 PE μA/>》f"3E&>EU9nηETP0E》ATEE>- NS%>A@μAμf 15% ~ 20% EA%eOBpμAEEtaDTTAE"42@yNo>-Tr0AAiE" V61≌μ¥qAOA1yNo>T↑/>>A≌E士E01aμtifμA 10% £国θδ EO0 PE %4o0μ2aEu3ETc ix/TEU26DA000坎②A1> TNSDOOAOi30 PE μA. ,B%4o0μD0E》XLPE tEO1- PE 0D。0°AμAA1> - °Ng)he0ED02-> -/kAxef"5&AlAT>-D0A0@AL61AEUAu3ujfECOf∩2/2>A≌96CiE ia. ,BEAIO> -)Aa&PE A EY/600|1e1e .PE %4-1e 1e1%》> A胆96OUEcTA14。. _δ_1kAxeμADOAUET -cEu中国煤化工:AEI)IT@TOOoμAta》- 9qo06%(1 iε60δ)a11ETμuA3a0S①AIEEDOAOIa_BYHCNMH GA"20hacLnyn mp.. L.gofA1>-%30}A}ia ,BE00E0U XLPE iaDi °6-0x024E1@2> EU2>EOTTEAIEEtEC0U 100c001AμAVT ,BAE qTsAUjE* E印QaE002000_04- 30.in 41 i@E0 AT200Ae μ0 6 E的"29 3i208y000T@μA1e fel}* A/VNEGYhoO0③μ%o0μD0A01>3A2i -0μuA-0x0A- EaEO"POESu<,1 iE0U0- 10A. y)%ix6CaXLPE VkawgCov6EUEAU∈WuOE3qCOOyEeAE' iP%+AUE4E3a>+Ci qE02ia. BEPE A- 0yEeuAijSijPCj@/u9fjPSijQOi @y4G>心[AE&1 aμξ%4σ 0μD0>nAE 1eNo>1e ie>1 ;E0OE1 Fa士iAxE6EEAOA:ODEula Bif土%Tpta>- 26u00E0E6RAμAWoσμ≥AATε3φCO%o0μD00U/2T ,B1 %>A0-A72318~7@TATE9IAiIuA>-NsSWeOEODE0AOtf30%T. BOμL2E0A0Uμc00D>u1yNo>- roy -cx+0ATA29-0D2> +¥9 1001@>uAAEAt12ajf910x0UE@yaμAleNo>oTa1UA01AμA1elelz00μu%z PE 0+A-④1YA1AINSDOAU06Ci126><6/k”E)>00 1r0UE@W°1e °N4E69T B>> VvAx+0ATA-C0E0U -0x0A~Val40EO》rNSA"CAETAIA:NSDOAO1a_BE-EuE@Wa2cE6°IDT3E i@ii@Oj5Si/>A@v/0$H' μA1e 1巨l》10+EC02作igO啡ialA¥DOjAlEataD0 i3B "cE"DOfktAB4U00TOjE- 0|E%ECTAL(2>ARATEO∪μ/3a∞≈E土2%》A2i -00%)>0/i9E2T ,BE1 V%》RO-OR一> 2RO" ."10~ CH2 CH2- CHr~~~+ RO"°→ ~~CH2 CH CH2~~~+ R一0H ."20~ CH2- -CH- -CH~~~+ H2C = CH- -S“0R2O - ~or CH2- - CH一 CH2~CH2- CH - -S" ORID"32@ .CH- -CH2- -S" ORfG+ p"°~m CH2- CH- CH2~"42@- ROHCH2- CH2- SLi" OREOCH2- CH2--Si- -OHORat~o CH2- CH- -CH2~ OR. H20~CH2- CH- CH2~ OR01CH2~~~"52⑥CH2-CH2 Si OHCH2- -CH2 Si0 SiCH2 CH2-: CHCH2~mf£" l£QE *35@/600|- 0|2*4ECE" 5f@l2>Aa .0!if2.3 0y-t%A20- 2AAT3E0AeE$EU1a 1min 仕-0aTA(ETa 160C ~ 200CuAOD>U1yNo>- TEEc1yNo》 Ip0i t0场" DCPf+71 Choey2.1340101p。BAOqE000~ HDPE2@pIAUqEy0U00IQ" LDPEOdBNo>- Ipio9i ie" DTBPE+93 CfFt23_-1p io9i >u1yNo>rDOuμTAOTE400TG LLDPEZODAOEW0007G MDPE200%。0i t02" 182 CE@E5-Tp/x>U-2E5 EE~ "Eaqi >1yNo>U200E ADE+79c&BiEaTi >1yNo>- }%x o宏" BPD£+66C£O2> i-AO作PE μA12>iTjfuEi{2.2 1ele2.4 i1N6%AA1A0ET29-0D0》δjE%00 μA00T0>i4° iEE@YaμAie4QF8: 1N516:; e+oni1/016310D1YATμAE*D0/°ORENo>ij@ENo>ij@+>i>oAEt UAU1AμA1e ie9uεEiEi/zACμ%Eμ3EF-μA中国煤化工/haja ,BE10AEUAUj&3EvEEUAEμAO@C6EAEOA0OTO>uUEyYxNo>i1ef@" VTMSE@100AμAO∪MHC N M H G.0BHTSQAE.EAO 01O>>uEy00No>u1e ie" VTESEOOIOUEy" 2-/x No >u00Nof"3-/x >0-6-Ea9i >Uth -02国EA2国° "3E5-Ea9li >-4-_C>u+%>ufDe [e" VTMES£00%N 3-/4x >utuTOoENo>Q+Q>0Eyl4xNo>u2@u Ea j34介i EA“们”" 10108甲dδ u TIp t0 a Ib 0A 106¥>u1eEE"VMMS历a0D VTMS E@YaEUE 60U26EyOBjCf'"DLTPfOUCAxEaEyEE>u+/6% ~TNPPEμE i1010 0o -0x0Ai@ 42E AT8w00016uA1e 1)>/w06;01002000Ae μ0 6 E白"29 Wi⑥vT6je0-cD0μi i和P%kj@P 10E%To. ,i320Arθe DLTP iExeAxe-0][TALni2j- -(E0%.8- -EEO|-KomAOEF.3ED- i-iaTμ0AOU XLPE的j&|Bxe-0| J2.5 y>Ax ^B>-WvA3.2 0.212-1003518E@)(a)>A@.-0lEaεEx0-cEpA胆“B> ~yAEO》°aE10AOD>uTyNOELTrEgMP1i >uTyIpOA1BEa6$uEjfy-cA2.6 -0Eφ%ABEU》m- →EOEU/4-36- .EEO; .- 20E-]EaAiμAEC%w0y -φ1Ajg1Nδ%AμE -01ai1Y0YVAGOE -0["B>-yA]Ec00 PE AEAT+1Axef3EOA;E0e PE IaEYμAμi -0x0Aε0°ia[i1NoyA340010Eq0qiaE A- uEjf|-0E$%A.310003.3 AU+OE/>i9T>01o0051°PE AEAT2j9- DCeE"1yNo》- Ip0i tQthkqpA1e1eE00e3.1 +>-/-1.0035-919>i9T%u0E960A0U>i 9[>u0D>iAqEz1 NO:%AI12>自B>-V4API0U>iA70UEU/aEoC°v0Eej£-"0! TAμf° 140 ~ 180CE国-1e e→[BEUxiqj→E:°0qk-38→0iAR→A xe-δ.0E%ahT3g° 5min ~ 30minf@贮3.4 μila12Q0μA1003518i3「-0Ec%A12r<2>t$9 i1eleyOEeμkEu2u LDPE μA. BN1-" 0|E+0D0e00T012306>> 6%0DDE@wx1)>>胆i&|1e °VE6°T|| ^B>-VA→+[ ,BEU,i→[EUEU/4.3]-→iAR- B xe-5][i1N6%A]「-0Ec%A]nCH2 = CH2+ CH2 = CH- S~ ORO一~CH2 CH2 CH CH2- CH2~m~ST"OREO42aE0-/-"-0etiO=E;38AaE 0AEO TAEθA -018 iE/3EEi W&" g国6AAE0%2j120 Ai 1- io °q3E 3u -1hBD1 Nu °0E00 Ib/4x th a EU%AE6U4.1 v:00|AEμA10281913j3EjEUDTEOEUx0O! uAV4- 38EONu&% A xe -0f% AaOA140caTAY1E; 6h26j36EONu°jfOe i0, E0Or0A9a0OL6j00i+0 "W0D2BU 90C eaTAYiEi 4h&Hu EONuAUT- y00;μA3δ%xE .3EAi iAE/E>AFE xE %国%L =&”W21eieμ$ia3eia。EX%>6;38EONva0U 80C9ae TaoDo∞jδ ,Eσr- wjfOW,i& 100% EWV所io91AEO%OEA&~ gfOW2但0. 5h26> 9640EEOE3E+jA2a369i ia1 alEx [14jZ0ATAEI/%NAE1-io iAEO%eTAyh°x0U0EA$^ *gfQEO=E 3%4YA+tax3M0>0+/kealoo0-aTuaEE G:G= L&" x/X2f@Ig" Y/Y26-ODE/SaEOOIEVAEa XLifXiQz -0t011 E4 i00+ 1uE0 -aμx2j0eq$2iμA1 1atE£-4.3 EaEDOAUAUqE" ρECB 1033-86E01a0. Eg" MFIECB 3682-83E>VTMS ):00!E+1uE0-a0U 1090cm-1" |&VTES 0U 1080cm~|&VTMES 00 1140cm-1|f-YjCY2 -040H1E%4 PE olA-EiG;qE" σ。f0:B 1040-79fTANEi3AE" ε% £CB 1040-79fimj中国煤化工79iE2030cm-1' |1uE0-aμx2i0e91$2iuA1 1atEtc y《“个%00|5 0°TMYHCN MHG .AEj£O=;E1"1y Heraeus 0≌E0 -0160C2aT"N69-AεEHo To%4FEEal/00lAEiE5.1 0-2AATμA0°Ti4.2 V>AqEqμA+106014j;85.1.1 PE μA00Aas5181-13i842>> A旦9oμAEONu00 800a ;0°aIaAU EOT 30min2-PEiE .01日HDPEjMIDPEj4DPEjCLDPEEGuAC0ONaiP43 i@E0 AT2000Ae μ0 6的"29 WiE .8y000T@μA1e fel}* A/VNEGYhoO0μACo+0/40⊥i 1if↑e PE ia1OAEA-EiCi TEiATEEDf+Gi 性2400! i*》A≌0eA-0%OxEi01 £θ/2ODA00U/>> A≌μA/zoDDEEgA "46EUA~Wa111eEOEU%uAUE1 Vkavg作TAVμi£>u0U00ET -0 i6EjE0000≌2200E-0xOAi -021W2W4000D000A0EpAIa, BE61/awsq作HDPEICDPE μ$qAE1 0AEtμAxU≌TD0AU2> EgFa12>iTYjEETEyrux)0U/00!91%> AEPE E0%a%WS .B401TiYaxSCox+0B%oDDAE' 6A;μAEμNei压al6a10%Q+i 21212+112> i-AUE PE μACot0Ai 1000 6140-x0x->uTAEyHDPEMDPELDPELLDPEE>心1.5Eal1w0-xOEyAii4x》uia8~4010~ 3500>0.5:.1140S》-作> LDPEAUOE2"g/cm3200. 940~0.9700.926~0.9400.910~0.9250.918~0.930wWawsnE/%85~ 95.75~8555~ 651c%$ '6Di/mm360390190412 2> 1-A0E PE y4°Ea1/> A@ATμAD0A0HDPE/LDPEHDPE/LLDPEIn AiLDPE| LDPE /%>A但AT HDPE HDPE />AAT| LLDPE2>AT1%>AAT6>ARATp2" gem?t0 0.9170.925.0.9510. 9660.918 .0. 9260. 9500.946MFIR" g/10min2@ 5.750.666.473.762.000.130.933.39σ。/MPa11.7611.0423.0027.8011.3212.5016.4619.02ε/% .495145100850014311124To/ C)011012349896XL/%i37.6817.23i934.8637.0077.20LLDPE OS>-EEEODEA AOO1γ2T°AE=T-Ni/>AOEEu5.1.2 1e160AAg5 714-1787De1eleAiE LDPEjCIDPE EUL-”0!E+Waq1i20U LLDPE μA1e1e0AAi q0%00.0|μAEUAE6°Ti1aAET≌rg= kg .1/须10D291uAWaWS社iE- -OEc0OU%.9δA-DoμA-G%°Ia f2"h:/h,60621i872 MiPAg ^600: .-0;EUAEsEy&ta个0DR0E 0U/600: μA1e 1e -0x00 a0u0u -q%4g IiaODf0o E0y -t)NA -0%a- 0! 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B00 XL la, ,BEC =0.5EXLjA-EiGirεEx0≌TA/oOBμAOAμa$p《LLDPE 06%40uμke0> g"aiqE士>咱惟TxT 6Et > 0.5Et y41Do la βTp0a0a£的↑s -EE+0E0UFEFEμ HDPE μAva%g2%μμ12> iTμAAUqE21E2>A00UA-Ei2i -0Ayz9zhaTμ0≥qE9U ' 6£6u00 -0x00Eq EOxeEAN0O-'GimEμAla, BiREaAaETβ HDPE: LLDPE = 80:20 E$XLjC .0| if1ele1yTaθEE -士1AxEδEfG&qETA/u$ayE02$%00!2,MFIjq TxT 6Ex09TD0AUxTYNjELLDPE W4U401μA XL y2T9%u0E2De0o40 DCP >ola. ,B-0| TAqECE 0O%:0AETrAT0UμI2p< LLDPE 0e HDPE 12>iEt XL E^90。BEAa>uAiEDTATi2AUE+puA/》AqEiE0ma1e1e0AAi 1~3 -YjfCa3pjf Elaf-00A0作PE uA MFI 2> 1-9q0D0A011025.1.3.0 msAoAA ;2i04147148174|*220" 6jfEc LDPE μA MFI , BE-0x0AiμizEuμAOEE-G;TEEDCIYH中国煤化工AEuA 1/2个weE6yμlεIFI μI∈GiTE0oEy_ ,BjE0-0oEC MFI μ1μA LDPE %4BODCN M H Go0200;i@》A∈EUAEOμAEai140- xO/2Tqja&61z0O;AEEEYG9qE%hT 6fPE A- x00E1402t iQL 06140生A- EiCi' (E06N0>)A+ 10LEi3s AEOO IAVyuE》>U2>0xAv°100012xE2AATE>njμAvT BμA XLiCi E00%°μ《DCP 6AA;1y”6>aμ40ATYAD03EETEyE61 y6OO!μ¥iax0A>-.30:A!;@AND0jf40°T2%pu1AE CjQXL 00V0EEAGM0-0|μAiOOEAUA|zh-Et.ia44石方数据E AT8w00016uA1e 1)>/w06;0102000Ae μ0 6 E白"29 Wi⑥>1 'oA- AEA: A0μuA36 iqiE0E0U0AAε 1yTaE- 0|4- 3610DAOAaTUE19 AE_BAODu0U>个> A0_ ,BμA- 0Y%oDD26u00B3E 1yTaμAiCi*Ci 4%>A+V/0261 XL 0Ue@%a/k》> A胆C° β。3TAODAOU/%> A胆j&iOOEAT i2c° qTTAqE 200C joq↑0U 40% 2613EDi taμAAsANjE0E0U%O0! jq2A曰. -0|>↑>-180Cj6q个160C jeul.190C2年/21AiTeμA/00! 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