Improved One-pot Synthesis of 4,6-Dihydroxyisophthalic Acid and 2,3-Dihydroxyterephthalic Acid
- 期刊名字:中国化学快报(英文版)
- 文件大小:
- 论文作者:Guang Dong LEI,Li Xin LI,Zhi Y
- 作者单位:College of Chemistry,Department of Chemistry and Life Science
- 更新时间:2022-12-23
- 下载次数:次
论文简介
An improved method for the large-scale preparation of 4,6-dihydroxyisophthalic acid and 2,3-dihydroxyterephthalic acid has been developed. Compared to the previous procedures,this new process requires much lower CO2 pressure of 0.3 Mpa and shorter reaction time, thus providing a convenient access for large-scale synthesis. The yield is high (93% and 65%,respectively), and the oxidation of phenol is nearly inhibited, neither decolorization nor further chromatographic purification is required.
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